Elucidation of glycolipid structure by proton nuclear magnetic resonance spectroscopy.
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Summary
The primary structure of the oligosaccharide moiety of a glycosphingolipid can be elucidated by employing high-field proton nuclear magnetic resonance (NMR) spectroscopy and a variety of one- and two-dimensional techniques are presented.
- Type
- review
- Published
- 1986-12-15
- Cited by
- 50
- References
- 42
- OpenAlex
- https://openalex.org/W2033672687
- Semantic Scholar
- https://api.semanticscholar.org/CorpusID:30913380
Keywords
Chemistry, Oligosaccharide, Nuclear magnetic resonance spectroscopy, Moiety, Glycosphingolipid
References
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- Specificity of binding of a strain of uropathogenic Escherichia coli to Gal alpha 1----4Gal-containing glycosphingolipids.
- Complete structural analysis of globoseries glycolipids by two-dimensional nuclear magnetic resonance.
- High-resolution proton NMR studies of gangliosides. 2. Use of two-dimensional nuclear Overhauser effect spectroscopy and sialylation shifts for determination of oligosaccharide sequence and linkage sites.
- Exploring nuclear spin systems by relayed magnetization transfer
- A Study of Methyl β-Xylobioside: An Illustrative Example of Two-Dimensional NMR Methods
- The conformational properties of the gangliosides GM2 and GM1 based on 1H and,13C nuclear magnetic resonance studies
- 1H-NMR-Untersuchungen an Sialinsäuren, V1 N-Acetyl-α-D-Neuraminsäure: Chemische Verschiebungen und Kopplungskonstanten; Konfiguration und Konformation in Lösung
- Improved spectral resolution in cosy 1H NMR spectra of proteins via double quantum filtering.
- Two-dimensional relayed coherence transfer spectroscopy of a protein
- Molecular parameters and conformation of globoside and asialo-GM1.
- Multiple quantum filters for elucidating NMR coupling networks
- 1H-NMR assignments of GM1-oligosaccharide in deuterated water at 500 MHz by two-dimensional spin-echo J-correlated spectroscopy.
- RESOLUTION AND ASSIGNMENT OF THE 270-MHZ PROTON SPECTRUM OF CELLOBIOSE BY HOMO-NUCLEAR AND HETERONUCLEAR TWO-DIMENSIONAL NMR
- Two‐dimensional spectroscopy. Application to nuclear magnetic resonance
- The conformations of oligosaccharides related to the ABH and Lewis human blood group determinants
Cited by
- Complex Carbohydrates in Drug Development
- 1H nuclear magnetic resonance spectroscopy of carbohydrate chains of glycoproteins.
- Structural analysis of oligosaccharides and glycoconjugates using NMR.
- Structural studies of lipopolysaccharides expressed by non-typeable Haemophilus influenzae and Haemophilus parainfluenzae strains
- Effect of trehalose on the viability of sporangiospores of the mucorous fungus Blakeslea trispora
- Structural elucidation of the Brucella melitensis M antigen by high-resolution NMR at 500 MHz.
- Structure of a novel sulfate-containing mycobacterial glycolipid.
- Advances on the compositional analysis of glycosphingolipids combining thin-layer chromatography with mass spectrometry.
- Interactions of sugars with membranes.
- Simple Construction of Neu5Ac(α2-8)Neu5Ac and Total Synthesis of Ganglioside GD3
- High‐Resolution Proton Magnetic Resonance Spectroscopy of Rabbit Brain: Regional Metabolite Levels and Postmortem Changes
- Carbohydrate epitope structural elucidation by 1H-NMR spectroscopy of a new Mycobacterium kansasii phenolic glycolipid antigen.
- High-resolution thin-layer chromatography of gangliosides.
- A synthetic approach to polysialogangliosides containing alpha-sialyl-(2-->8)-sialic acid: total synthesis of ganglioside GD3.
- Gangliosides, Ab1 and Ab2 antibodies I. Towards a molecular dissection of an idiotype-anti-idiotype system.
- Structures of glucolipids from the membrane of Acholeplasma laidlawii strain A-EF22. I. Glycerophosphoryldiglucosyldiacylglycerol and monoacylbisglycerophosphoryldiglucosyldiacylglycerol.
- Structures of glucolipids from the membrane of Acholeplasma laidlawii strain A-EF22. III. Monoglucosyldiacylglycerol, diglucosyldiacylglycerol, and monoacyldiglucosyldiacylglycerol.
- Novel type-specific lipooligosaccharides from Mycobacterium tuberculosis.
- Wild Type Rhizobium etli, a Bean Symbiont, Produces Acetyl-fucosylated, N-Methylated, and Carbamoylated Nodulation Factors (*)
- Scalar, dipolar-correlated and J-resolved 2D-NMR spectroscopy of the specific phenolic mycoside of Mycobacterium tuberculosis.
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